DOI: 10.1007/s13369-019-03808-8 Corpus ID: 108841189; Understanding the Reaction Mechanism of Lithium–Sulfur Batteries by In Situ/Operando X-ray Absorption Spectroscopy
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AI Customer ServiceAn integrated three-stage adsorption process was designed and evaluated to maximize the recovery of lithium from SLR. Results presented in Fig. 7 imply that the adsorption on both adsorbent granules decreased in subsequent adsorption stages, likely due to the reduced concentration gradient.
Lithium recovery from spent lithium-ion battery raffinate was investigated. Pretreatment of the raffinate removed 84% of organics and improved Li extraction. Mn and Al-based adsorbents exhibited excellent Li adsorption behavior. Adsorption kinetics, capacity, and selectivity suggest high technical feasibility.
The lithium adsorption/desorption capacity assessed in every cycle is presented in Fig. 9. The adsorbents exhibited relatively stable performance, with adsorption capacities fluctuating around 4.5 mg/g for Mn-based adsorbent and 3.5 mg/g for Al-based adsorbent across the cycles.
Lithium/aluminum layered double hydroxides (Li/Al-LDHs) without elution damage, have been regarded as the most applicable adsorbents in the industrial lithium extraction from brines, while the low adsorption capacity and unclear adsorption/desorption mechanism are restraining their lithium extraction performance.
There are three main types of inorganic metal-based lithium ion adsorbents extensively applied for lithium extraction, including layered Al-based adsorption materials, Mn-based ion sieves, and Ti-based ion sieves , . The lithium adsorption process of these metal-based ion sieves is mainly governed by structural memory effect .
Both Mn and Al-based adsorbent granules exhibited rapid adsorption of lithium from the pretreated SLR, reaching saturation within 2 h, with final capacity in the range 4–5 mg of lithium per g of adsorbent granular material.
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